Abstract According to the time context, the chemical experiment teaching of high school in our country was divided into four main stages. The first stage was to learn from the Soviet Union, grope forward period. With the birth of new China, Chinese new educational system has been gradually established. From the Ministry of Education promulgated the first Outline, the status of high school chemical experiment teaching was established and continued to this day. This period of high school chemical experiment teaching for students mastering "Shuangji" played a more important role. The second stage was the encounter "the great cultural revolution" destruction of the retrogression period, many times "movement" caused the shock to the high school chemical experiment teaching, once stagnant.