Design of Comprehensive Experiment for Isoprene Coordination PolymerizationCatalyzed by Transition
LIU Wen-Jing1, GUO Li-Hua1, XU Shuai1, LIU Yan-Lan1, LI Qin-Yu2
1. School of Chemistry and Chemical Engineering, Qufu Normal University, Qufu 273165, China;
2. The Open Sharing Service Platform of Instrument and Equipment, Qufu Normal University, Qufu 273165, China
Abstract The pyridineimine iron and cobalt complexes have been synthesized and investigated as precatalysts for isoprene polymerization in the presence of dichloroethyl aluminum as a cocatalyst. The microstructure of the obtained polymer was also characterized by nuclear magnetic resonance (NMR) and infrared spectroscopy(IR). This experiment covers three aspects of organic synthesis, complex synthesis and polymer synthesis, which is conducive to the comprehensive training of students' experimental skills.
LIU Wen-Jing, GUO Li-Hua, XU Shuai, LIU Yan-Lan, LI Qin-Yu. Design of Comprehensive Experiment for Isoprene Coordination PolymerizationCatalyzed by Transition[J]. Chinese Journal of Chemical Education, 2018, 39(10): 39-43.
