Abstract According to the time context, the chemical experiment teaching of high school in our country was divided into four main stages. The third stage was "bring order out of chaos", the rapid development period, accompanied by "the great cultural revolution" ending, the convening of The Third Plenary Session of the 11th Central Committee of CPC, Chinese education has ushered in a new era of development. In this historical period, the high school chemical experiment teaching revolved around the center of the country, the educational function had been continuously expanded, the teaching quality has been improved continuously. In the teaching practice, some new teaching ideas and teaching methods had been produced, the teachers' competence had been improved continuously, and the experimental teaching theory also got development.