Abstract This paper introduces an innovative teaching experiment that integrates the scanning electrochemical microscopy(SECM)into the comprehensive experimental curriculum for undergraduate majors,aiming to bridge the gap between basic education and cutting-edge scientific research.This experiment systematically elaborates the imaging principle of SECM,guides students to undertake tasks such as the preparation,characterization,and preliminary application experiments involving ultramicroelectrodes,demonstrates the operational principles of SECM,and instructs students to conduct data analysis.By integrating SECM technology into experimental teaching,it not only enriches the experimental content,improves students' understanding of electrochemical knowledge,but also develops their experimental skills and innovative thinking.This paper demonstrates the potential of SECM in education and scientific research,provides a forward-thinking practical platform for nurturing future talents in the renewable energy sector.
HUI Jing-Shu, TANG Ji-Gui, WANG Zi-Ming, WU Ze. Exploring the Mysteries of Microscopic Electrochemistry:Scanning Electrochemical Microscopy in Undergraduate Teaching Experiment[J]. Chinese Journal of Chemical Education, 2025, 46(16): 63-69.